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板栗殼中原花青素大孔吸附樹(shù)脂分離純化工藝優(yōu)化
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國(guó)家自然科學(xué)基金資助項(xiàng)目(309700309)、國(guó)家博士后基金資助項(xiàng)目(20100471379)、江蘇省高校自然基金資助項(xiàng)目(05KJB550011)、江蘇大學(xué)人才基金資助項(xiàng)目(05JDG013、128300289)和江蘇高校優(yōu)勢(shì)學(xué)科建設(shè)工程資助項(xiàng)目


Separation and Purification Procyanidins from Chestnut-shells by Macroporous Resin
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    摘要:

    比較了12種大孔吸附樹(shù)脂對(duì)板栗殼中原花青素的吸附與解吸性能，在靜態(tài)吸附研究基礎(chǔ)上，篩選出效果較好的樹(shù)脂進(jìn)行動(dòng)態(tài)試驗(yàn)，并對(duì)所得組分原花青素含量及其相對(duì)分子量進(jìn)行分析。結(jié)果表明，AB-8大孔吸附樹(shù)脂分離純化CSPCs效果最佳，上樣質(zhì)量濃度為1.864mg/mL，流速為2 mL/min；當(dāng)用體積分?jǐn)?shù)為50%乙醇以1 mL/min的流速洗脫4個(gè)柱體積時(shí)，CSPCs 的累積回收率可達(dá)94.2 %，含量為89.8%。經(jīng)質(zhì)譜分析，分子量范圍為289.4~1154.9，聚合度在4以?xún)?nèi)。

    Abstract:

    With the aim to separate and purify procyanidins from chestnut-shells (CSPCs) by macroporous resin, twelve macroporous resins were tested for their static adsorption/desorption performance towards CSPCs. Based on the static adsorption experiments, the suitable macroporous resin was screened to carry out dynamic adsorption experiment, the content and the relative molecular weight of CSPCs were analyzed. The results showed that AB-8 was the optimal macroporous resin for separating and purifying CSPCs, the optimum separating condition was as follows: the mass concentration and the sampling rate were 1.864 mg/mL and 2 mL/min, respectively. The total recovery of CSPCs reached 94.2% eluted with 50% ethanol of 4 BV at a flow velocity of 1 mL/min, and the content of the total CSPCs in the obtained fine product was 89.8%. Analysis of CSPCs by ESI-MS demonstrated the molecular weight ranged from 289.4 to 1154.9 (M+H) within 4 of average polymeric degree.

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張海暉,段玉清,李金鳳,馬海樂(lè),邵婷婷,徐菲菲.板栗殼中原花青素大孔吸附樹(shù)脂分離純化工藝優(yōu)化[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2011,42(5):156-159,155. Zhang Haihui, Duan Yuqing, Li Jinfeng, Ma Haile, Shao Tingting, Xu Feifei. Separation and Purification Procyanidins from Chestnut-shells by Macroporous Resin[J]. Transactions of the Chinese Society for Agricultural Machinery,2011,42(5):156-159,155.

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